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The reduction of the azido group was performed twice in a mixture of 1,4-dioxane/H 2 O (7:3 v/v) (5 mL) with a 1 M PMe 3 solution in THF (10 equiv) under microwave irradiation (50 C, 50 W, 30 min)
Cold medications straight from the refrigerator take longer to warm in winter if your home runs cool
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